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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1673444Erstellt: 26. Oktober 2026

Tert-butyl 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoate → 4-(Benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoic acid

https://huagongshe.com/reaction/1673444

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTert-butyl 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoateHCID 67342913—
LösungsmittelTrifluoroacetic acidHCID 6422—
Produkt4-(Benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoic acidHCID 57879410—

Reaktionsschritte

10 mL of trifluoroacetic acid was added to the obtained tert-butyl 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoate and stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure and methanol was added to the obtained residue and a solid substance was separated by filtration to obtain 31 mg of 4-(benzo[1,3]dioxol-5-yl)-2-(2,3-dimethylbenzamido)benzoic acid as white solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07999132B2
Quelldatensatzuspto-grants-2011_08
ORD IDord-9aa7eda3a966471e8efde12db1382b51
Quellennotizuspto-grants-2011_08