HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromo-4-methoxybutane → Phenazine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromo-4-methoxybutane | HCID 521168 | — |
| Edukt | 1-Phenazinol | HCID 135412648 | — |
| Produkt | Phenazine | HCID 4757 | — |
| Produkt | Ethoxyethane;phenazine | HCID 67351390 | — |
Reaktionsschritte
Scheme 6 illustrates the synthesis of N-ethyl phenazine 1-hydroxybutyl methyl ether. The phenazine ether (21) is prepared by the alkylation of the 1-hydroxyphenazine (1) with 4-methoxybutylbromide (Aldrich Chemical Company, USA) to give phenazine derivative (21). N-ethyl phenazine (22) is prepared by reaction of compound (21) with diethyl sulfate in the presence of potassium carbonate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08008037B2 |
| Quelldatensatz | uspto-grants-2011_08 |
| ORD ID | ord-272dd0f606174ba689283296606922c8 |
| Quellennotiz | uspto-grants-2011_08 |