Diethylamine → HCID 15951003, Verbindung
Reaktionsgleichung
F[C:2]1[CH:7]=[CH:6][C:5]([C:8]([N:10]2[CH2:14][CH2:13][CH2:12][CH:11]2[CH2:15][N:16]2[CH2:20][CH2:19][CH2:18][CH2:17]2)=[O:9])=[CH:4][CH:3]=1.[CH2:21]([NH:23][CH2:24][CH3:25])[CH3:22]>>[CH2:21]([N:23]([CH2:24][CH3:25])[C:2]1[CH:7]=[CH:6][C:5]([C:8]([N:10]2[CH2:14][CH2:13][CH2:12][C@H:11]2[CH2:15][N:16]2[CH2:20][CH2:19][CH2:18][CH2:17]2)=[O:9])=[CH:4][CH:3]=1)[CH3:22]Komponenten
3
Versuchsvorschrift
(4-Diethylamino-phenyl)-(2-(S)-pyrrolidin-1-ylmethyl-pyrrolidin-1-yl)-methanone is prepared from (4-Fluoro-phenyl)-(2-pyrrolidin-1-ylmethyl-pyrrolidin-1-yl)-methanone and diethylamine in a manner substantially similar to Procedure A. MS (APCI+) 330 (M+H)+.
Quellen und Nachweise
- ORD-Eintrag
- ord-12dbdf3a87254f069ee9f06fa69b5175
- Quelldatensatz
- uspto-grants-2011_08
- Patentnummer