3-Nitro-4-(trifluoromethoxy)benzoic acid → 3-Amino-4-(trifluoromethoxy)benzoic acid
Reaktionsgleichung
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[O:13][C:14]([F:17])([F:16])[F:15])[C:7]([OH:9])=[O:8])([O-])=O>CO>[NH2:1][C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[O:13][C:14]([F:15])([F:16])[F:17])[C:7]([OH:9])=[O:8]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
A solution of 3-nitro-4-trifluoromethoxybenzoic acid (3 g) in methanol (240 ml) was hydrogenated at 50° C. and 50 bar using H-cube apparatus. The methanol solution was evaporated giving the title compound as a white solid (2.58 g).
Aufarbeitung
- customwas hydrogenated at 50° C.
- customThe methanol solution was evaporated
Quellen und Nachweise
- ORD-Eintrag
- ord-ebfd23b88677408e80c4208b95b8ebd6
- Quelldatensatz
- uspto-grants-2011_08
- Patentnummer
- US08008303B2
Notizen zur Reaktion
Wird geladen…