(+-)-4-Methylhexanoic acid → HCID 12600624, Verbindung

Reaktionsgleichung

[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5](O)=[O:6].S(Cl)([Cl:12])=O>>[CH3:1][CH:2]([CH2:8][CH3:9])[CH2:3][CH2:4][C:5]([Cl:12])=[O:6]

Komponenten

Edukt 2

HCID 15271(+-)-4-Methylhexanoic acid

HCID 24386Thionyl Chloride

Produkt 1

HCID 12600624HCID 12600624, Verbindung

Versuchsvorschrift

The acid from step A2 is converted into the acid chloride by interaction with thionyl chloride according to a standard method. After removal of the excess of thionyl chloride, the residual acid chloride is used in step C2 without further purification.

Aufarbeitung

customAfter removal of the excess of thionyl chloride
customthe residual acid chloride is used in step C2 without further purification

Quellen und Nachweise

ORD-Eintrag: ord-677e682bdd7c48c3b1e43681e0ff2d2d
Quelldatensatz: uspto-grants-1978_03
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04077260

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