HCID 178463890, Verbindung → HCID 178463877, Verbindung

HRID 1679267Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1679267
[OH:1][C:2]1[CH:7]=[C:6]([CH2:8]C(O)=O)[N:5]=[C:4]([N:12]([CH2:15][CH3:16])[CH2:13][CH3:14])[N:3]=1>C(O)C>[OH:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]=[C:4]([N:12]([CH2:13][CH3:14])[CH2:15][CH3:16])[N:3]=1

Komponenten

3

Edukt 1

HCID 178463890HCID 178463890, Verbindung

Produkt 1

HCID 178463877HCID 178463877, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

4-Hydroxy-2-diethylaminopyrimidin-6-yl acetic acid (4.0 g) was suspended in ethanol (50 ml) and the mixture refluxed for 16 hours. The volatile portion of the mixture was then evaporated under reduced pressure to yield 4-hydroxy-2-diethylamino-6-methyl pyrimidine as a white powder, melting at 135° C.

Aufarbeitung

  1. temperaturethe mixture refluxed for 16 hours
  2. customThe volatile portion of the mixture was then evaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-3f7a19b4e9aa45d08b52f63ed0edecf2
Quelldatensatz
uspto-grants-1978_03
Patentnummer
US04080326

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