1,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl- → HCID 70575974, Verbindung

HRID 1679495Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1679495
[Cl:1]N1C(=O)NC(=O)N(Cl)C1=O.[Na].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][N:15]1[CH3:23]>CO>[Cl-:1].[O:13]=[C:14]1[N:19]([CH3:20])[C:18](=[O:21])[N:17]([CH3:22])[CH2:16][NH+:15]1[CH3:23]

Komponenten

4

Edukt 2

HCID 1816881,3,5-Triazinane-2,4-dione, 1,3,5-trimethyl-HCID 86657659Sodium dichlorocyanuric acid

Produkt 1

HCID 70575974HCID 70575974, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

17.8 g (0.1 mol) of sodium dichlorocyanuric acid are added to 15.7 g (0.1 mol) of 2,4-dioxo-hexahydro-1,3,5-trimethyl-s-triazine in 50 ml of methanol and the mixture is stirred. The cyanuric acid which has precipitated is then filtered off and the filtrate is evaporated. The residue which remains on evaporation is digested with water. After renewed filtration to remove residual cyanuric acid, an aqueous solution of the same compound as in Example g is obtained.

Aufarbeitung

  1. customThe cyanuric acid which has precipitated
  2. filtrationis then filtered off
  3. customthe filtrate is evaporated
  4. customThe residue which remains on evaporation
  5. filtrationfiltration
  6. customto remove residual cyanuric acid
  7. customan aqueous solution of the same compound as in Example g is obtained

Quellen und Nachweise

ORD-Eintrag
ord-3769b7e41fcb49179062e8fdcf5f8766
Quelldatensatz
uspto-grants-1978_03
Patentnummer
US04080502

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