Ethanol → 3-Methyl-4-(prop-2-en-1-yl)-1-(alpha-methyl-3,4-di-chlorobenzyl)-pyrazol-5-one

Beteiligte Stoffe

Reaktionsschritte

17 g (0.1 mol) of allylacetoacetic acid ethyl ester were added to a mixture of 20.5 g of α-methyl-3,4-dichorobenzylhydrazine and 30 ml of absolute ethanol under nitrogen, whereupon the temperature rose to 55° C. The reaction mixture was heated to the reflux temperature for 2 hours. After cooling, the reaction product crystallized out

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