Pyrrolidine → HCID 23454971, Verbindung
Reaktionsgleichung
N1CCCC1.C(NNC1(N=C=S)C=CC=CC1)=O.[CH:19]([NH:21][NH:22][C:23]1[CH:28]=[CH:27][C:26]([NH:29][C:30]([N:32]([CH2:40][C:41]2[CH:46]=[CH:45]C=CC=2)CC2C=CC=CC=2)=[S:31])=[CH:25][CH:24]=1)=[O:20]>>[CH:19]([NH:21][NH:22][C:23]1[CH:24]=[CH:25][C:26]([NH:29][C:30]([N:32]2[CH2:40][CH2:41][CH2:46][CH2:45]2)=[S:31])=[CH:27][CH:28]=1)=[O:20]Komponenten
4
Versuchsvorschrift
Pyrrolidine (0.071 g, 0.001 mole) and 1-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.15 g (58 percent), m.p. 199°-201° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-9efc38b06dfd4dd18f52ba090da51e72
- Quelldatensatz
- uspto-grants-1981_06
- Patentnummer
- US04276364
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