3-Pyrroline → HCID 23454968, Verbindung

Reaktionsgleichung

N1CC=CC1.C(NNC1(N=C=S)C=CC=CC1)=O.[CH:19]([NH:21][NH:22][C:23]1[CH:28]=[CH:27][C:26]([NH:29][C:30]([N:32]([CH2:40][C:41]2[CH:46]=[CH:45]C=CC=2)CC2C=CC=CC=2)=[S:31])=[CH:25][CH:24]=1)=[O:20]>>[CH:19]([NH:21][NH:22][C:23]1[CH:24]=[CH:25][C:26]([NH:29][C:30]([N:32]2[CH2:40][CH:41]=[CH:46][CH2:45]2)=[S:31])=[CH:27][CH:28]=1)=[O:20]

Komponenten

Edukt 3

HCID 660593-Pyrroline

HCID 23454956HCID 23454956, Verbindung

HCID 23454969HCID 23454969, Verbindung

Produkt 1

HCID 23454968HCID 23454968, Verbindung

Versuchsvorschrift

3-Pyrroline (0.069 g, 0.001 mole) and 1-(2-formylhydrazino)phenyl isothiocyanate (0.19 g, 0.001 mole) were reacted according to the procedure described for NA-11 in Example 3. Yield 0.18 g (69 percent), m.p. 218°-220° C.

Quellen und Nachweise

ORD-Eintrag: ord-9547ce2a39e745c9a2f9fc6fc3108cdf
Quelldatensatz: uspto-grants-1981_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04276364

Notizen zur Reaktion

Wird geladen…