Methanol → HCID 14880138, Verbindung

HRID 1681025Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1681025
[CH3:1][O:2][CH2:3][O:4][CH2:5][C:6]#[N:7].[Na].[CH3:9][OH:10]>>[CH3:1][O:2][CH2:3][O:4][CH2:5][C:6](=[NH:7])[O:10][CH3:9]

Komponenten

4

Edukt 3

HCID 887MethanolHCID 5360545SodiumHCID 19736216(Methoxymethoxy)acetonitrile

Produkt 1

HCID 14880138HCID 14880138, Verbindung

Versuchsvorschrift

Obtained using the procedure described in section a of Example 2, starting with 286.8 g (2.84 moles) of methoxymethoxyacetonitrile [prepared according to D. J. Loder and W. M. Bruner, U.S. Pat. No. 2,398,757; C.A. 1946, 40, 3774] and 6.5 g (0.284 gram-atom) of sodium in 1430 ml of methanol. Reaction time: 2 days. Yld: 302.6 g (80%), b.p.15 16°-65° C.

Aufarbeitung

  1. customObtained
  2. customprepared
  3. customReaction time
  4. custom2 days
  5. custom302.6 g (80%), b.p.15 16°-65° C.

Quellen und Nachweise

ORD-Eintrag
ord-b653f3cf2c8b430c906fa2dfc6772b64
Quelldatensatz
uspto-grants-1992_12
Patentnummer
US05167949

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