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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1690676Erstellt: 26. Oktober 2026

2-(3,5-Dimethyl-4-propoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane → 9-(3,5-Dimethyl-4-propoxy-phenyl)-10-fluoro-5,11-dihydro-6H-benzo[a]carbazole-3-carboxylic acid methyl ester

https://huagongshe.com/reaction/1690676

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt2-(3,5-Dimethyl-4-propoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolaneHCID 57618490—
Edukt9-Chloro-10-fluoro-5,11-dihydro-6H-benzo[a]carbazole-3-carboxylic acid methyl esterHCID 66904663—
Produkt9-(3,5-Dimethyl-4-propoxy-phenyl)-10-fluoro-5,11-dihydro-6H-benzo[a]carbazole-3-carboxylic acid methyl esterHCID 16048341—

Reaktionsschritte

A sample of crude 9-Chloro-10-fluoro-5,11-dihydro-6H-benzo[a]carbazole-3-carboxylic acid methyl ester (prepared as in example 57, step 2) and 2-(3,5-Dimethyl-4-propoxy-phenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane are coupled as in example 19, step 2 to afford the title material: ESMS m/z/z 458 (M+H+).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08153671B2
Quelldatensatzuspto-grants-2012_04
ORD IDord-2f028fe06a5b405788387a72a416f1d8
Quellennotizuspto-grants-2012_04