HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylamine → 5-(Dimethylamino)-2-nitrobenzoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylamine | HCID 674 | — |
| Edukt | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| Produkt | 5-(Dimethylamino)-2-nitrobenzoic acid | HCID 12715793 | — |
Reaktionsschritte
Concretely, 5-chloro-2-nitrobenzoic acid is dissolved in a dimethylamine aqueous solution and heated to produce 5-dimethylamino-2-nitrobenzoic acid. Hydrochloric acid is added to the reaction solution to precipitate out the product as a solid material. The solid material is separated to obtain 5-dimethylamno-2-nitrobenzoic acid almost quantitatively.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07737274B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-d83951711c72435a9bf755e0eb273d0b |
| Quellennotiz | uspto-grants-2010_06 |