3,4-Dimethoxyphenylboronic acid → tert-Butyl [(5-chloro-3',4'-dimethoxybiphenyl-2-yl)oxy]acetate
Reaktionsgleichung
[C:1]([O:5][C:6](=[O:17])[CH2:7][O:8][C:9]1[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][C:10]=1Br)([CH3:4])([CH3:3])[CH3:2].[CH3:18][O:19][C:20]1[CH:21]=[C:22](B(O)O)[CH:23]=[CH:24][C:25]=1[O:26][CH3:27]>>[Cl:15][C:12]1[CH:13]=[CH:14][C:9]([O:8][CH2:7][C:6]([O:5][C:1]([CH3:4])([CH3:3])[CH3:2])=[O:17])=[C:10]([C:23]2[CH:22]=[CH:21][C:20]([O:19][CH3:18])=[C:25]([O:26][CH3:27])[CH:24]=2)[CH:11]=1Komponenten
3
Versuchsvorschrift
The subtitle compound was prepared by the method of example 1 step (ii) using the product from example 1 step (i) and 3,4-dimethoxyphenylboronic acid. Yield 0.86 g
Quellen und Nachweise
- ORD-Eintrag
- ord-b159cb6f7b744aaea513622bbd3e76e2
- Quelldatensatz
- uspto-grants-2012_04
- Patentnummer