Isoamyl Nitrite → 2-Chloro-4-(ethylthio)-1-iodo-benzene

Beteiligte Stoffe

Reaktionsschritte

A solution of 3-chloro-4-iodo-aniline (5.6 g), isoamylnitrite (8.8 ml) and ethyldisulphide (13.4 ml) in acetonitrile (100 ml) was heated at 60° C. for 24 h. The solvent was removed under reduced pressure and the residue purified by chromatography on silica eluting with 1% ethylacetate/isohexane. Yield 4.02 g

Herkunft & Nachweise