1-Butanone, 1-(4-hydroxyphenyl)- → HCID 67276722, Verbindung

HRID 1696694

Reaktionsgleichung

Reaktionsgleichung von HRID 1696694
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8][CH:9]([CH3:29])[C:10]([C:12]1[CH:17]=[CH:16][C:15]([O:18][Si:19]([CH:26]([CH3:28])[CH3:27])([CH:23]([CH3:25])[CH3:24])[CH:20]([CH3:22])[CH3:21])=[CH:14][CH:13]=1)=[O:11].O[C:31]1C=CC(C(=O)CCC)=CC=1>>[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[S:8][CH:9]([CH2:29][CH3:31])[C:10]([C:12]1[CH:17]=[CH:16][C:15]([O:18][Si:19]([CH:23]([CH3:25])[CH3:24])([CH:26]([CH3:28])[CH3:27])[CH:20]([CH3:21])[CH3:22])=[CH:14][CH:13]=1)=[O:11]

Komponenten

3

Edukt 2

HCID 660921-Butanone, 1-(4-hydroxyphenyl)-HCID 672774092-[(2-Hydroxyphenyl)thio]-1-{4-[(triisopropylsilyl)oxy]phenyl}propan-1-one

Produkt 1

HCID 67276722HCID 67276722, Verbindung

Versuchsvorschrift

The intended compound was obtained according to the method of Reference Example 1-1-(1), (2), (3), according to a method similar to it, and according to a combination of the method with an ordinary method, but using 4′-hydroxybutyrophenone as the starting material. 1HNMR (400 MHz, CDCl3, ppm): 1.02-1.19 (18H, m), 1.21-1.32 (3H, m), 1.80-2.05 (211, m), 4.36 (1H, t, J=6.9 Hz), 6.77-7.02 (4H, m), 7.22-7.37 (2H, m), 7.77-7.79 (2H, m)

Aufarbeitung

  1. customThe intended compound was obtained

Quellen und Nachweise

ORD-Eintrag
ord-dd61deb917344bb8ae5a73d6fbc21cca
Quelldatensatz
uspto-grants-2012_04
Patentnummer
US08163770B2

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