HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(Oxan-4-yl)hydrazine hydrochloride → HCID 67278257, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (Oxan-4-yl)hydrazine hydrochloride | HCID 17773358 | — |
| Edukt | (2S,4R)-methyl 4-(2-chlorophenylsulfonyl)-1-(3-oxobutanethioyl)pyrrolidine-2-carboxylate | HCID 86646820 | — |
| Produkt | HCID 67278257 | HCID 67278257 | — |
Reaktionsschritte
In analogy to the procedure described in example 192 h, (2S,4R)-methyl 4-(2-chlorophenylsulfonyl)-1-(3-oxobutanethioyl)pyrrolidine-2-carboxylate (example 253c) was reacted with (tetrahydropyran-4-yl)hydrazine hydrochloride (CAS Reg. No. 194543-22-1) to give the title compound as orange oil. MS (ESI): m/z=468.1 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08163793B2 |
| Quelldatensatz | uspto-grants-2012_04 |
| ORD ID | ord-5ae75c660d8c4646b1f350476e9a947e |
| Quellennotiz | uspto-grants-2012_04 |