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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1698450Erstellt: 26. Oktober 2026

Piperonal → Bis(3,4-methylenedioxy)chalcone

https://huagongshe.com/reaction/1698450

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPiperonalHCID 8438—
EduktSodium HydroxideHCID 14798—
EduktAcetopiperoneHCID 76622—
LösungsmittelEthanolHCID 702—
ProduktBis(3,4-methylenedioxy)chalconeHCID 294346—

Reaktionsschritte

A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08163957B2
Quelldatensatzuspto-grants-2012_04
ORD IDord-6e2fb4f5e95948368cd6489babc13cc7
Quellennotizuspto-grants-2012_04