Hydrochloric Acid → 5-Nitro-indan-2-ylamine hydrochloride
Reaktionsgleichung
C([NH:4][CH:5]1[CH2:13][C:12]2[C:7](=[CH:8][CH:9]=[C:10]([N+:14]([O-:16])=[O:15])[CH:11]=2)[CH2:6]1)(=O)C.[ClH:17]>>[ClH:17].[N+:14]([C:10]1[CH:11]=[C:12]2[C:7](=[CH:8][CH:9]=1)[CH2:6][CH:5]([NH2:4])[CH2:13]2)([O-:16])=[O:15]Komponenten
3
Versuchsvorschrift
N-Acetyl-5-nitro-2-indanamine, 1.5 g. (0.007 mole) as prepared in Example 9 was refluxed in 10% hydrochloric acid for 3 hours. The mixture was evaporated and the crystalline residue recrystallized from methanol-ether to yield 5-nitro-2-indanamine hydrochloride, dec.>280° C.
Aufarbeitung
- custom(0.007 mole) as prepared in Example 9
- customThe mixture was evaporated
- customthe crystalline residue recrystallized from methanol-ether
Quellen und Nachweise
- ORD-Eintrag
- ord-00640c1748ab49b6be035facddf7563e
- Quelldatensatz
- uspto-grants-1980_03
- Patentnummer
- US04192888
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