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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1701494Erstellt: 25. Oktober 2026

4,5-Dichloro-2-methylaniline → 5-Chloro-2-methylaniline

https://huagongshe.com/reaction/1701494

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4,5-Dichloro-2-methylanilineHCID 343796—
LösungsmittelHydrochloric AcidHCID 313—
LösungsmittelWaterHCID 962—
Produkt5-Chloro-2-methylanilineHCID 726082%

Reaktionsschritte

Following the general procedure I, 0.25 mol of 4,5-dichloro-2-methylaniline in 200 ml of water and 60 ml of concentrated hydrochloric acid are hydrogenated in the presence of the catalyst from Example 1 at 220° C. over the course of 30 minutes under a hydrogen pressure of 100 atmospheres gauge. 5-Chloro-2-methylaniline is obtained in a yield of 82% and a purity of 99%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04193937
Quelldatensatzuspto-grants-1980_03
ORD IDord-8037112fe81848e297759b0be669a25f
Quellennotizuspto-grants-1980_03