HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Salicylamide → 2-Propoxybenzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Salicylamide | HCID 5147 | — |
| Edukt | 1-Iodopropane | HCID 33643 | — |
| Edukt | Sodium Methoxide | HCID 10942334 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 2-Propoxybenzamide | HCID 43051 | — |
Reaktionsschritte
A 130 gm portion of salicylamide in 500 ml. of ethanol is reacted with 52.4 gm. of sodium methoxide and 164.9 gm. of 1-iodopropane by heating at reflux. The mixture is cooled, precipitated in 1500 ml. of water and the solid is recrystallized from hot ethanol giving o-propoxybenzamide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04124766 |
| Quelldatensatz | uspto-grants-1978_11 |
| ORD ID | ord-1c15088dbfb145e3b4a7f93c176ad759 |
| Quellennotiz | uspto-grants-1978_11 |