Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1703850Erstellt: 26. Oktober 2026

Bromo-4'-chloro-3'-sulfamoylacetophenone → 3-Ethyl-4-(4-chloro-3-sulfamoylphenyl)-2-isopropylimino-1,3-thiazolidine-4-ol-hydrochloride

https://huagongshe.com/reaction/1703850

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBromo-4'-chloro-3'-sulfamoylacetophenoneHCID 12952390—
Edukt1-Ethyl-3-isopropylthioureaHCID 19650595—
LösungsmittelAcetoneHCID 180—
Produkt3-Ethyl-4-(4-chloro-3-sulfamoylphenyl)-2-isopropylimino-1,3-thiazolidine-4-ol-hydrochlorideHCID 22760539—

Reaktionsschritte

6.2 g of 2-bromo-4'-chloro-3'-sulfamoylacetophenone and 2.92 g of 1-ethyl-3-isopropylthiourea were heated in 40 ml of acetone for 15 minutes to 40° C., the mixture was stirred for another 30 minutes at room temperature and the crystals were filtered. Colorless crystalline solid body: melting point: 188° C. (decomposition).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04125614
Quelldatensatzuspto-grants-1978_11
ORD IDord-584a2bac8be64985bd13627ad0065a54
Quellennotizuspto-grants-1978_11