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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1704356Erstellt: 25. Oktober 2026

Ethyl 3-oxovalerate → Diethyl 2-Propionylazelate

https://huagongshe.com/reaction/1704356

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthyl 3-oxovalerateHCID 78656—
EduktEthyl 7-bromoheptanoateHCID 122490—
EduktMethyl 8-Ethoxycarbonyl-9-oxo-5-decynoateHCID 22759276—
ProduktDiethyl 2-PropionylazelateHCID 22759291—

Reaktionsschritte

The synthesis of this compound is carried out by the procedure of Example 4, Step A, except that an equivalent quantity of ethyl propionylacetate is substituted for the ethyl acetoacetate of Example 4, Step A, and an equivalent quantity of ethyl 7-bromoheptanoate is substituted for the methyl 7-bromo-5-heptynoate of Example 4, Step A. The product, a viscous oil, is used in the next step directly without distillation.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04126629
Quelldatensatzuspto-grants-1978_11
ORD IDord-b40bd894bfd64ceba0582cf8f7b08c27
Quellennotizuspto-grants-1978_11