HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenyl Isothiocyanate → N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenyl Isothiocyanate | HCID 7673 | — |
| Edukt | 4-chloro-N-cyclopentylbenzylamine | HCID 834083 | — |
| Produkt | N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea | HCID 13018271 | 92,8% |
Reaktionsschritte
Analogously to Example 1, 21 grams (0.1 mole) of N-4-chlorobenzyl-N-cyclopentylamine were reacted with 13.5 grams (0.1 mole) of phenylisothiocyanate. 32 grams of N-4-chlorobenzyl-N-cyclopentyl-N'-phenylthiourea were obtained. Yield: 92%, Melting point: 129°-132° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04127673 |
| Quelldatensatz | uspto-grants-1978_11 |
| ORD ID | ord-c45d45730c5d4b50b13b1fe0493dcdd3 |
| Quellennotiz | uspto-grants-1978_11 |