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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1706345Erstellt: 25. Oktober 2026

Chlorine → Butanamide, 2-chloro-N-methyl-3-oxo-

https://huagongshe.com/reaction/1706345

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktChlorineHCID 24526—
EduktN-MethylacetoacetamideHCID 88483—
ProduktButanamide, 2-chloro-N-methyl-3-oxo-HCID 2006597,4%

Reaktionsschritte

Altogether, the aqueous phase was subjected to chlorination five times. A total of 492 parts by weight of N-methylacetoacetamide (MMAA) of 99.5% strength, and 283.5 parts by weight of chlorine were used, and altogether 588.6 parts by weight of 97.4% N-methyl-α-chloracetoacetamide (MMCAA) were obtained, that is, 96.8% of the theoretical yield, calculated on reacted MMAA.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04207259
Quelldatensatzuspto-grants-1980_06
ORD IDord-98d701b02df64754a597f1c35a67078e
Quellennotizuspto-grants-1980_06