1-Bromo-3-methylbutane → HCID 18963351, Verbindung
Reaktionsgleichung
[C:1]([C:4]1[CH2:9][CH2:8][CH2:7][NH:6][CH:5]=1)(=[O:3])[CH3:2].Br[CH2:11][CH2:12][CH:13]([CH3:15])[CH3:14]>>[CH3:14][CH:13]([CH3:15])[CH2:12][CH2:11][N:6]1[CH2:7][CH2:8][CH2:9][C:4]([C:1]([CH3:2])=[O:3])=[CH:5]1Komponenten
3
Versuchsvorschrift
Methyl 1-(3-methylbutyl)-1,4,5,6-tetrahydro-3-pyridyl ketone was prepared from 3-acetyl-1,4,5,6-tetrahydropyridine and 1-bromo-3-methylbutane according to the procedure of Part b) of Example 1. The product distilled as a pale yellow oil (b.pt. 103°-106° C./0.1 mm Hg).
Aufarbeitung
- distillationThe product distilled as a pale yellow oil (b.pt. 103°-106° C./0.1 mm Hg)
Quellen und Nachweise
- ORD-Eintrag
- ord-e0c95c9795544f9a938ced4f4985c55b
- Quelldatensatz
- uspto-grants-1994_10
- Patentnummer
- US05352793
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