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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1709083Erstellt: 24. Oktober 2026

Lithium Chloride → 3-Chloro-1,1,1,2,2-Pentafluoropropane

https://huagongshe.com/de/reaction/1709083

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktLithium ChlorideHCID 433294—
Edukt2,2,3,3,3-Pentafluoropropyl p-ToluenesulfonateHCID 2776017—
LösungsmittelN-methyl-2-pyrrolidoneHCID 13387—
Produkt3-Chloro-1,1,1,2,2-PentafluoropropaneHCID 67905—

Reaktionsschritte

These solvents are readily prepared from commercially available materials by standard and well-known organic syntheses techniques. For example, to prepare 1,1-dichloro-2,2,3,3,3-pentafluoropropane, 2,2,3,3,3-pentafluoro-1-propanol and p-toluenesulfonate chloride are reacted together to form 2,2,3,3,3-pentafluoropropyl-p-toluenesulfonate. Then, N-methylpyrrolidone, lithium chloride, and the 2,2,3,3,3-pentafluoropropyl-p-toluenesulfonate are reacted together to form 1-chloro-2,2,3,3,3-pentafluoropropane. Chlorine and the 1-chloro-2,2,3,3,3-pentafluoropropane are then reacted together to form 1,1-dichloro-2,2,3,3,3-pentafluoropropane.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04947881
Quelldatensatzuspto-grants-1990_08
ORD IDord-a6395cafc7654f769fc718ecaff0dc8b
Quellennotizuspto-grants-1990_08