HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,1,3-Trichloro-1,2,2,3,3-pentafluoropropane → 1,3-Dichloro-1,1,2,2,3-pentafluoropropane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,1,3-Trichloro-1,2,2,3,3-pentafluoropropane | HCID 74244 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | 1,3-Dichloro-1,1,2,2,3-pentafluoropropane | HCID 62353 | — |
Reaktionsschritte
For example, to prepare 1,3-dichloro-1,1,2,2,3-pentafluoropropane, 2,2,3,3-tetrafluoropropanol, tosyl chloride, and water are reacted together to form 2,2,3,3-tetrafluoropropyl p-toluenesulfonate. Then, N-methylpyrrolidone, potassium fluoride, and the 2,2,3,3-tetrafluoropropyl p-toluenesulfonate are reacted together to form 1,1,2,2,3-pentafluoropropane. Then, chlorine and the 1,1,2,2,3-pentafluoropropane are reacted to form 1,1,3-trichloro-1,2,2,3,3-pentafluoropropane. Finally, isopropanol and the 1,1,3-trichloro-1,2,2,3,3-pentafluoropropane are reacted to form 1,3-dichloro-1,1,2,2,3-pentafluoropropane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04947881 |
| Quelldatensatz | uspto-grants-1990_08 |
| ORD ID | ord-add53b74b1bb42179fb853d922c7fbad |
| Quellennotiz | uspto-grants-1990_08 |