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HRID 1709086Erstellt: 26. Oktober 2026

1,1,3-Trichloro-1,2,2,3,3-pentafluoropropane → 1,3-Dichloro-1,1,2,2,3-pentafluoropropane

https://huagongshe.com/reaction/1709086

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1,1,3-Trichloro-1,2,2,3,3-pentafluoropropaneHCID 74244—
LösungsmittelIsopropanolHCID 3776—
Produkt1,3-Dichloro-1,1,2,2,3-pentafluoropropaneHCID 62353—

Reaktionsschritte

For example, to prepare 1,3-dichloro-1,1,2,2,3-pentafluoropropane, 2,2,3,3-tetrafluoropropanol, tosyl chloride, and water are reacted together to form 2,2,3,3-tetrafluoropropyl p-toluenesulfonate. Then, N-methylpyrrolidone, potassium fluoride, and the 2,2,3,3-tetrafluoropropyl p-toluenesulfonate are reacted together to form 1,1,2,2,3-pentafluoropropane. Then, chlorine and the 1,1,2,2,3-pentafluoropropane are reacted to form 1,1,3-trichloro-1,2,2,3,3-pentafluoropropane. Finally, isopropanol and the 1,1,3-trichloro-1,2,2,3,3-pentafluoropropane are reacted to form 1,3-dichloro-1,1,2,2,3-pentafluoropropane.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04947881
Quelldatensatzuspto-grants-1990_08
ORD IDord-add53b74b1bb42179fb853d922c7fbad
Quellennotizuspto-grants-1990_08