HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → (Pyridin-2-ylsulfanyl)-acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Methyl 2-pyridin-2-ylsulfanylacetate | HCID 15388132 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | (Pyridin-2-ylsulfanyl)-acetic acid | HCID 654661 | 95% |
Reaktionsschritte
A solution of the ester from above (751 mg, 4.10 mmol) in MeOH (50 ml) and 1N NaOH (10 ml) was stirred at room temperature for 45 minutes to give (pyridin-2-ylsulfanyl)-acetic acid (655 mg, 95%) after acidic work-up.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07790747B2 |
| Quelldatensatz | uspto-grants-2010_09 |
| ORD ID | ord-2253ce553bff44268f3d42805d563042 |
| Quellennotiz | uspto-grants-2010_09 |