Allyl bromide → 4-Allyloxy-3-nitrobenzaldehyde

HRID 1712252

Reaktionsgleichung

[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11].[CH2:13](Br)[CH:14]=[CH2:15]>>[CH2:15]([O:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11])[CH:14]=[CH2:13]

Komponenten

Edukt 2

HCID 7841Allyl bromide

HCID 181694-Hydroxy-3-nitrobenzaldehyde

Produkt 1

HCID 224011524-Allyloxy-3-nitrobenzaldehyde

Versuchsvorschrift

Analogously to Method F, 25 g of 4-hydroxy-3-nitrobenzaldehyde and 25.1 ml of allyl bromide are reacted. The title compound is obtained as a slightly yellowish solid. Rf=0.30 (1:2 EtOAc-heptane). Rt=4.00.

Quellen und Nachweise

ORD-Eintrag: ord-1c9822a86c62464eb41a7a1ef5f32e09
Quelldatensatz: uspto-grants-2010_09
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07790715B2

Verknüpfte Notizen

Wird geladen…