HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formaldehyde → 2,3,4-Trihydroxy-5-(pyrrolidin-1-ylmethyl)benzaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formaldehyde | HCID 712 | — |
| Edukt | Pyrrolidine | HCID 31268 | — |
| Edukt | 2,3,4-Trihydroxybenzaldehyde | HCID 75064 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 2,3,4-Trihydroxy-5-(pyrrolidin-1-ylmethyl)benzaldehyde | HCID 59235875 | — |
Reaktionsschritte
17.1 g (0.24 mol) of pyrrolidine were added to 19.2 g (0.24 mol) of a 37% aqueous formaldehyde solution in 140 ml of ethanol. Then 25.0 g (0.16 mol) of 2,3,4-trihydroxybenzaldehyde were added thereto. The reaction mixture was refluxed for one hour, developing a dark brown color. After cooling, a beige-brown solid precipitated out, which was filtered out and dried.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07799096B2 |
| Quelldatensatz | uspto-grants-2010_09 |
| ORD ID | ord-67d55e0849d94d16add0d304b338eac5 |
| Quellennotiz | uspto-grants-2010_09 |