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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1720375Erstellt: 26. Oktober 2026

(3,4-Dichlorophenoxy)acetic acid → HCID 18603269, Verbindung

https://huagongshe.com/reaction/1720375

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(3,4-Dichlorophenoxy)acetic acidHCID 11495—
EduktCyclohexanamine, N-methyl-2-(1-pyrrolidinyl)-, trans-HCID 13377463—
ProduktHCID 18603269HCID 18603269—

Reaktionsschritte

The title compound was prepared according to the method described in Example 2, using 3,4-dichlorophenoxyacetic acid (2.34 g, 11 mmol) and (±)-trans-N-methyl-N-[2-(1-pyrrolidinyl)cyclohexyl]amine prepared in Example 1 (2 g, 11 mmol). The crude product, which started to precipitate before the addition of the diethyl ether, was recrystallised from hot dichloromethane. Yield 2.9 g (62%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05506257
Quelldatensatzuspto-grants-1996_04
ORD IDord-f450219564a54cf28b79e61e172337c4
Quellennotizuspto-grants-1996_04