Ethanol → Ethyl sulfoacetate

HRID 1721388

Reaktionsgleichung

Reaktionsgleichung von HRID 1721388
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

Komponenten

3

Edukt 2

HCID 702EthanolHCID 31257Sulfoacetic acid

Produkt 1

HCID 12216623Ethyl sulfoacetate

Versuchsvorschrift

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

Aufarbeitung

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

Quellen und Nachweise

ORD-Eintrag
ord-25099fe8278a4bf3ab4105d4b60c77d8
Quelldatensatz
uspto-grants-1996_04
Patentnummer
US05510379

Verknüpfte Notizen

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