Thionyl Chloride → HCID 20025664, Verbindung

HRID 1723408Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1723408
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([OH:19])=O)=[CH:5][CH:4]=1.S(Cl)([Cl:22])=O>C(Cl)Cl>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([Cl:22])=[O:19])=[CH:5][CH:4]=1

Komponenten

4

Edukt 2

HCID 24386Thionyl ChlorideHCID 14555669HCID 14555669, Verbindung

Produkt 1

HCID 20025664HCID 20025664, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel

Versuchsvorschrift

To an ice-cold, stirring solution of 3 gm 9(4-methoxyphenyl)nonanoic acid in 10 ml. CH2Cl2 was added dropwise 1.2 ml thionyl chloride. The solution was then allowed to warm up to room temperature. The solvent and excess thionyl chloride were removed in vacuo to give a brown oil, which was used directly in the last step without further purification.

Aufarbeitung

  1. customThe solvent and excess thionyl chloride were removed in vacuo
  2. customto give a brown oil, which
  3. customwas used directly in the last step without further purification

Quellen und Nachweise

ORD-Eintrag
ord-aab12e7043bc497c8d1a1db10757b098
Quelldatensatz
uspto-grants-1989_08
Patentnummer
US04861798

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