Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 2,4,5-Trifluorobenzoyl chloride | HCID 145164 | — |
| Edukt | Ethyl 3-(cyclopentylamino)buta-2-enoate | HCID 66962611 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | HCID 178472172 | HCID 178472172 | — |
Reaktionsschritte
Under ice cooling, triethylamine and 2,4,5-trifluorobenzoyl chloride were added to a solution of ethyl 3-(cyclopentylamino)buta-2-enoate in dioxane, for stirring at ambient temperature for 30 minutes and at 65° C. for one hour, to obtain ethyl 3-(cyclopentylamino)-2-(2,4,5-trifluorobenzoyl)buta-2-enoate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US07488739B2 |
|---|
| Quelldatensatz | uspto-grants-2009_02 |
|---|
| ORD ID | ord-a74a10861c204c4ea7edab78d2610844 |
|---|
| Quellennotiz | uspto-grants-2009_02 |
|---|
