HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Lactitol dihydrate → Lactulose
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Lactitol dihydrate | HCID 157354 | — |
| Edukt | Lactitol Monohydrate | HCID 3067270 | — |
| Produkt | Lactulose | HCID 11333 | — |
Reaktionsschritte
Examples XII-XXVII elucidate the conditions at which lactitol monohydrate and lactitol dihydrate, respectively, may be obtained from aqueous solutions of lactitol. In each instance 200 g lactitol dihydrate was used as the starting material which wasd dissolved in an amount of water varying from 40 g to 50 g at 100° C. Thereupon the solutions obtained were cooled to a temperature varying from 25° C. to 45° C. and seeded with 2 g monohydrate or 2 g dihydrate. The crystallization proper occurred at temperatures between 18° C. and 45° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05726303 |
| Quelldatensatz | uspto-grants-1998_03 |
| ORD ID | ord-3780dab8e7fc4abdb18faae656691afb |
| Quellennotiz | uspto-grants-1998_03 |