Azobisisobutyronitrile → 2-Ethylhexyl methacrylate-giycidyl methacrylate

HRID 1728529

Reaktionsgleichung

Reaktionsgleichung von HRID 1728529
[C:1]([O:6][CH2:7][CH:8]([CH2:13][CH3:14])[CH2:9][CH2:10][CH2:11][CH3:12])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:15]([O:20][CH2:21][CH:22]1[O:24][CH2:23]1)(=[O:19])[C:16]([CH3:18])=[CH2:17].N(C(C)(C)C#N)=NC(C)(C)C#N>>[CH2:21]([O:20][C:15](=[O:19])[C:16]([CH3:18])=[CH2:17])[CH:22]1[O:24][CH2:23]1.[C:1]([O:6][CH2:7][CH:8]([CH2:13][CH3:14])[CH2:9][CH2:10][CH2:11][CH3:12])(=[O:5])[C:2]([CH3:4])=[CH2:3]

Komponenten

4

Edukt 3

HCID 6547AzobisisobutyronitrileHCID 7837Glycidyl methacrylateHCID 127132-Ethylhexyl methacrylate

Produkt 1

HCID 867479712-Ethylhexyl methacrylate-giycidyl methacrylate

Versuchsvorschrift

To the above solvent, a mixture of 200 g of 2-ethylhexyl methacrylate, 10 g of glycidyl methacrylate and 3 g of azobisisobutyronitrile was added dropwise at a constant speed over a period of 3 hours, followed by stirring for 1 hour to complete the polymerization reaction. Thus, 2-ethylhexyl methacrylate - glycidyl methacrylate copolymer was obtained.

Aufarbeitung

  1. additionwas added dropwise at a constant speed over a period of 3 hours
  2. customthe polymerization reaction

Quellen und Nachweise

ORD-Eintrag
ord-b6f754cc209b4ca19e818c8f4fe9eee2
Quelldatensatz
uspto-grants-1994_07
Patentnummer
US05328794

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