Methyl iodide → 3-[[Acetyl[[4-(tetradecyloxy)phenyl]methyl]amino]methyl]-1-methylpyridinium iodide

HRID 1728853

Reaktionsgleichung

Reaktionsgleichung von HRID 1728853
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][N:8]([CH2:12][C:13]2[CH:18]=[CH:17][C:16]([O:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33])=[CH:15][CH:14]=2)[C:9](=[O:11])[CH3:10])[CH:2]=1.[CH3:34][I:35]>>[I-:35].[C:9]([N:8]([CH2:7][C:3]1[CH:2]=[N+:1]([CH3:34])[CH:6]=[CH:5][CH:4]=1)[CH2:12][C:13]1[CH:14]=[CH:15][C:16]([O:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH3:33])=[CH:17][CH:18]=1)(=[O:11])[CH3:10]

Komponenten

3

Edukt 2

HCID 6328Methyl iodideHCID 10026896N-(3-Pyridinylmethyl)-N-[[4-(tetradecyloxy)phenyl]methyl]acetamide

Produkt 1

HCID 100086413-[[Acetyl[[4-(tetradecyloxy)phenyl]methyl]amino]methyl]-1-methylpyridinium iodide

Versuchsvorschrift

The title compound is prepared by the procedure of Example 28 using 0.492 g of product from Example 73 and 3.38 ml of methyl iodide. The residue is purified by crystallization to give 0.64 g of the desired product as orange crystals.

Aufarbeitung

  1. customThe residue is purified by crystallization

Quellen und Nachweise

ORD-Eintrag
ord-923a49bdaa34455abc571962f0509609
Quelldatensatz
uspto-grants-1994_07
Patentnummer
US05328921

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