Methyl iodide → HCID 53635658, Verbindung

HRID 1729102Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1729102
[CH3:1][C:2]([C:25]([O:27][CH3:28])=[O:26])([CH2:17][C:18]1[CH:23]=[CH:22][C:21]([OH:24])=[CH:20][CH:19]=1)[NH:3][C:4]([O:6][CH:7]1[CH:14]2[CH2:15][CH:10]3[CH2:11][CH:12]([CH2:16][CH:8]1[CH2:9]3)[CH2:13]2)=[O:5].[C:29](=O)([O-])[O-].[K+].[K+].IC>>[CH3:29][O:24][C:21]1[CH:20]=[CH:19][C:18]([CH2:17][C:2]([CH3:1])([C:25]([O:27][CH3:28])=[O:26])[NH:3][C:4]([O:6][CH:7]2[CH:8]3[CH2:16][CH:12]4[CH2:11][CH:10]([CH2:15][CH:14]2[CH2:13]4)[CH2:9]3)=[O:5])=[CH:23][CH:22]=1

Komponenten

4

Edukt 3

HCID 6328Methyl iodideHCID 11430Potassium CarbonateHCID 54546551HCID 54546551, Verbindung

Produkt 1

HCID 53635658HCID 53635658, Verbindung

Versuchsvorschrift

The title compound was prepared from methyl α-methyl-N-[(tricyclo[3.3.1.13,7 ]dec-2-yloxy)carbonyl]-DL-tyrosinate (0.671 g, 0.0017 mmol, prepared usingthe procedure described in Example 47, Step A), potassium carbonate (0.345 g, 0.0025 mmol) and iodomethane (0.368 g, 0.0025 mol) using the procedure described in Example 47, Step B. MS: 402.4 (MH+).

Aufarbeitung

  1. customprepared usingthe procedure

Quellen und Nachweise

ORD-Eintrag
ord-ed91aaf59da7444c9518261f37f98c1b
Quelldatensatz
uspto-grants-1994_07
Patentnummer
US05331006

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