HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethylamine → 4-Ethylamino-3-nitrobenzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethylamine | HCID 6341 | — |
| Edukt | 4-Chloro-3-nitrobenzamide | HCID 27942 | — |
| Produkt | 4-Ethylamino-3-nitrobenzamide | HCID 3708922 | — |
Reaktionsschritte
II (160 g - 0.8 mole) was added portionwise with stirring at 60° C to 720 g of 50 % by weight aqueous ethylamine. The mixture was cooled, the precipitate was collected and crystallized from the monomethyl ether of ethylene glycol (5 ml per gram of dried product).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03989522 |
| Quelldatensatz | uspto-grants-1976_11 |
| ORD ID | ord-bb3097a7e15a44488e01fcb467723d81 |
| Quellennotiz | uspto-grants-1976_11 |