HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Miconazole → HCID 178521218, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Miconazole | HCID 4189 | — |
| Edukt | 2,4-Dichloro-alpha-(chloromethyl)benzenemethanol | HCID 94351 | — |
| Lösungsmittel | Benzonitrile | HCID 7505 | — |
| Produkt | HCID 178521218 | HCID 178521218 | — |
Reaktionsschritte
4.2 parts of 1-[2,4-dichloro-β-(2,4-dichlorobenzyloxy)phenethyl]imidazole and 3 parts of 2,4-dichloro-α-(chloromethyl)benzyl alcohol are mixed together in 40 parts of benzonitrile and the resulting mixture is stirred at reflux temperature for 3 days. At the end of this period the reaction solvent is evaporated off under reduced pressure to obtain a 1-[2,4-dichloro-β-(2,4-dichlorobenzyloxy)phenethyl]-3-(2,4dichloro-β-hydroxyphenethyl)imidazolium chloride product as residue.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03991202 |
| Quelldatensatz | uspto-grants-1976_11 |
| ORD ID | ord-b8c99004b2fc46d8abdd7b201cc6f99d |
| Quellennotiz | uspto-grants-1976_11 |