HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ammonia → N,N-Dimethylaminopropyl acrylamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ammonia | HCID 222 | — |
| Edukt | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 3-Hydroxypropanamide | HCID 4145140 | — |
| Produkt | N,N-Dimethylaminopropyl acrylamide | HCID 77452 | — |
Reaktionsschritte
59.3 g of β-hydroxypropionic acid amide and 68 g of 3-dimethylaminopropylamine were heated for 5 hours in a temperature range of 125°-168° C. until the evolution of ammonia was complete. After adding 1 g of pulverised sodium hydroxide the reaction mixture was distilled.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04237067 |
| Quelldatensatz | uspto-grants-1980_12 |
| ORD ID | ord-9fb2048b1977420aad17c78493b3ea51 |
| Quellennotiz | uspto-grants-1980_12 |