Aniline → 2-Butylmercaptoaniline

HRID 1732822

Reaktionsgleichung

Reaktionsgleichung von HRID 1732822
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[SH:10])([O-])=O.N[C:12]1[CH:17]=CC=[CH:14][CH:13]=1.C(N1CCCC1=O)O.ClCC(Cl)=O>>[CH2:17]([S:10][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[NH2:1])[CH2:12][CH2:13][CH3:14]

Komponenten

5

Edukt 4

HCID 6115AnilineHCID 6577Chloroacetyl chlorideHCID 21002o-NitrobenzenethiolHCID 849112-Pyrrolidinone, 1-(hydroxymethyl)-

Produkt 1

HCID 103299602-Butylmercaptoaniline

Versuchsvorschrift

2-Butylmercaptoaniline was prepared from -2-nitrothiophenol by a two-step reaction sequence consisting of alkylation followed by reduction corresponding to the procedure described in Example 4. The aniline then was condensed with N-methylolpyrrolidone, followed by reaction with chloroacetyl chloride to yield the desired product.

Aufarbeitung

  1. customby a two-step reaction sequence

Quellen und Nachweise

ORD-Eintrag
ord-9bb7ea5ee3214d5ca67c785aa455bc90
Quelldatensatz
uspto-grants-1980_12
Patentnummer
US04239688

Verknüpfte Notizen

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