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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1733514Erstellt: 27. Oktober 2026

Chloroform → 3-[4-(Hexadecylamino)benzoyl]-4-carboethoxythiazolidine

https://huagongshe.com/reaction/1733514

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktChloroformHCID 6212—
EduktTriethylamineHCID 8471—
EduktEthyl thiazolidine-4-carboxylateHCID 103574—
Edukt4-Hexadecylaminobenzoyl chloride hydrochlorideHCID 13255322—
LösungsmittelDichloromethaneHCID 6344—
Produkt3-[4-(Hexadecylamino)benzoyl]-4-carboethoxythiazolidineHCID 20437342—

Reaktionsschritte

One-tenth mole of 4-(hexadecylamino)benzoyl chloride hydrochloride in methylene chloride is added to a solution of 0.1 mole of ethyl thiazolidine-4-carboxylate in chloroform containing two equivalents of triethylamine. After 5 hours at 20° C. the solution is filtered and evaporated to a white solid which is recrystallized from acetonitrile.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04242273
Quelldatensatzuspto-grants-1980_12
ORD IDord-b438f0a10e6a44a6be7e4ba64147f148
Quellennotizuspto-grants-1980_12