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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1733574Erstellt: 25. Oktober 2026

Hydrazine → 5-(4-Chlorophenyl)-2-hydrazinopyridine

https://huagongshe.com/reaction/1733574

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrazineHCID 9321—
Edukt2-Chloro-5-(4-chlorophenyl)pyridineHCID 10036554—
LösungsmittelPyridineHCID 1049—
Produkt5-(4-Chlorophenyl)-2-hydrazinopyridineHCID 20300092—

Reaktionsschritte

A mixture of 21.1 g. of 2-chloro-5-(4-chlorophenyl)pyridine and 19.5 g. of 95% hydrazine in 200 ml. of pyridine is heated at reflux temperature for 48 hours. The reaction mixture is cooled, poured into an ice-water mixture and filtered. The solid is collected, washed with water and air dried to yield 17.0 g. of the product of the Example as a tan solid.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04242515
Quelldatensatzuspto-grants-1980_12
ORD IDord-48403d4dbc804813a861d5cc9eae947e
Quellennotizuspto-grants-1980_12