Ammonia → Allyl anthranilate

HRID 1736361Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1736361
[N+:1]([C:4]1[CH:15]=[CH:14][CH:13]=[CH:12][C:5]=1[C:6]([O:8][CH2:9][CH:10]=[CH2:11])=[O:7])([O-])=O.C(OC1C=C(C=CC=1[N+]([O-])=O)C(OCC=C)=O)C=C.N>>[NH2:1][C:4]1[CH:15]=[CH:14][CH:13]=[CH:12][C:5]=1[C:6]([O:8][CH2:9][CH:10]=[CH2:11])=[O:7]

Komponenten

4

Edukt 3

HCID 222AmmoniaHCID 13788700Allyl 2-nitrobenzoateHCID 19432478Allyl 3-allyloxy-4-nitrobenzoate

Produkt 1

HCID 24116Allyl anthranilate

Versuchsvorschrift

The above nitro compound was reduced by the method described in example 1, for the reduction of allyl 3-allyloxy-4-nitrobenzoate, except using an aqueous solution of ammonia in place of sodium bicarbonate in the work-up, to give allyl 2-aminobenzoate.

Quellen und Nachweise

ORD-Eintrag
ord-537ae6ed13b34a329726b4872ed45441
Quelldatensatz
uspto-grants-1996_07
Patentnummer
US05541178

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