HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Adamantanone → N'-(adamantan-2-ylidene)(tert-butoxy)carbohydrazide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Adamantanone | HCID 64151 | — |
| Edukt | tert-Butyl carbazate | HCID 70091 | — |
| Lösungsmittel | Hexane | HCID 8058 | — |
| Produkt | N'-(adamantan-2-ylidene)(tert-butoxy)carbohydrazide | HCID 8039095 | — |
Reaktionsschritte
A hexane solution containing 2-adamantanone (2 g) and tert-butyl carbazate (1.76 g) was heated to reflux for 3 hours. When the solution cooled, the title compound crystallized and was filtered (3.28 g). M.p. 175-177°
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05962496 |
| Quelldatensatz | uspto-grants-1999_10 |
| ORD ID | ord-fde0bd09b7b94d7b8dfc18b83e4509a4 |
| Quellennotiz | uspto-grants-1999_10 |