3,5-Di-tert-butylcatechol → 1,2-Bis-(2-cyanophenoxy)-3,5-di-tert-butylbenzene

HRID 1739346Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1739346
F[C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#[N:5].[OH:10][C:11]1[CH:16]=[C:15]([C:17]([CH3:20])([CH3:19])[CH3:18])[CH:14]=[C:13]([C:21]([CH3:24])([CH3:23])[CH3:22])[C:12]=1[OH:25]>>[C:4]([C:3]1[CH:6]=[CH:7][CH:8]=[CH:9][C:2]=1[O:10][C:11]1[CH:16]=[C:15]([C:17]([CH3:18])([CH3:19])[CH3:20])[CH:14]=[C:13]([C:21]([CH3:24])([CH3:23])[CH3:22])[C:12]=1[O:25][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#[N:5])#[N:5]

Komponenten

3

Edukt 2

HCID 660993,5-Di-tert-butylcatecholHCID 678552-Fluorobenzonitrile

Produkt 1

HCID 218407351,2-Bis-(2-cyanophenoxy)-3,5-di-tert-butylbenzeneAusbeute 90,1 %

Versuchsvorschrift

The compound 1,2-bis-(2-cyanophenoxy)-3,5-di-tert-butylbenzene was prepared, according to the procedure of Example 1, by reacting 2-fluorobenzonitrile with 1,2-dihydroxy-3,5-di-tert-butyl benzene. The product was recrystallized from ethanol to give a 90.1% yield of the title compound with the formula: ##STR12##

Aufarbeitung

  1. customThe compound 1,2-bis-(2-cyanophenoxy)-3,5-di-tert-butylbenzene was prepared
  2. customThe product was recrystallized from ethanol

Quellen und Nachweise

ORD-Eintrag
ord-16e603754d8a40d0b3aeca6c6f6dc4a7
Quelldatensatz
uspto-grants-1999_10
Patentnummer
US05965690

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