HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Nitric Acid → 4-Amino-3-nitropyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Nitric Acid | HCID 944 | — |
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 4-Aminopyridine | HCID 1727 | — |
| Edukt | 2-Nitropyridin-3-amine | HCID 83281 | — |
| Edukt | Propanenitrile, 2-amino- | HCID 411840 | — |
| Produkt | 4-Amino-3-nitropyridine | HCID 548803 | — |
Reaktionsschritte
4-Amino-3-nitropyridine was synthesized by a literature reference [Harris M. G. and Stewart R. Can. J. Chem. 55, 3800 (1977)]; by nitration of 4-aminopyridine with conc. sulfuric acid and fuming nitric acid. This aminonitropyridine was then converted to the aminopropionitrile derivative IV by the method described in Example 1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05968946 |
| Quelldatensatz | uspto-grants-1999_10 |
| ORD ID | ord-43f197b3e3d046e6af821251aff2b1c6 |
| Quellennotiz | uspto-grants-1999_10 |