1-Bromo-3-chloropropane → (3-Chloropropyl)hexyldimethylammonium bromide
Reaktionsgleichung
[CH3:1][N:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:3].[Br:10][CH2:11][CH2:12][CH2:13][Cl:14]>CO>[Br-:10].[Cl:14][CH2:13][CH2:12][CH2:11][N+:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])([CH3:3])[CH3:1]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Reaktionsbedingungen
- Temperatur
- 65 °C
Versuchsvorschrift
A 500 mL, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-dimethylhexylamine (199.46 grams, 1.54 moles), 1-bromo-3-chloropropane (243.00 grams, 1.54 moles) and 250 mL of methanol. The reaction was maintained at 65° C. for 24 hours. Solvent was removed by rotary evaporation under reduced pressure to yield a brown, viscous oil. Yield 445.8 grams (1.55 moles, 100%).